The Art of Process Chemistry
The Art of Process Chemistry内容简介
Providing must-have knowledge for the pharmaceutical industry and process chemists in industry, this ready reference offers solutions for saving time and money and supplying -- in a sustainable way -- valuable products. Application-oriented and well structured, each chapter presents successful strategies for the latest modern drugs, showing how to provide very fast bulk quantities of drug candidates. Throughout, the text illustrates how all the key factors are interwoven and dependent on one another in creating optimized methods for optimal products.
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Epimerization of the α- position of the aldehyde was observed at 2∼4% when the reaction mixture was quenched into water. This epimerization was totally prevented by quenching into phosphate buffer.
It was found that when 3 was left standing in CH2Cl2 for long period [22] , which was the solvent for the next step, it reacted with solvent to form dimer 52, together with formation of the HCl salt of 3.
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